Synthesis and characterization of various surfactants for stabilized CuO powder

Synthesis and characterization of various surfactants for stabilized CuO powder

Alina MATEI, Vasilica ŢUCUREANU, Marian POPESCU, Cosmin ROMANIŢAN, Bogdan BIŢĂ, Ileana CERNICA

Abstract: In the present work, CuO nanoparticles were successfully prepared by the coprecipitation method using copper acetate (Cu(CH3COO)2) as a basic precursor, sodium hydroxide (NaOH) as a precipitator material, sodium dodecyl sulfate (SDS) and cetyltrimethylammonium bromide (CTAB) as anionic and cationic surfactants, respectively. The synthesized powders samples were characterized by Fourier transform infrared spectrometry (FT-IR), field emission scanning electron microscopy (FESEM) and X-ray diffraction (XRD). The investigation showed that the added types of surfactants have effects on the decrease of the crystallite size, on the CuO particles morphology, shape and uniform distribution as it is noticed in the XRD and SEM characterizations. Additionally, the FTIR spectra for all the powders samples showed the same Cu-O stretching vibration mode which indicates the presence of a crystalline CuO monoclinic structure. The obtained results create premises for further advanced the applications of CuO powders in various domains.

Keywords
Copper oxide, Nanoparticles, Surfactants, Chemical method

Published online 11/5/2018, 9 pages
Copyright © 2018 by the author(s)
Published under license by Materials Research Forum LLC., Millersville PA, USA

Citation: Alina MATEI, Vasilica ŢUCUREANU, Marian POPESCU, Cosmin ROMANIŢAN, Bogdan BIŢĂ, Ileana CERNICA, ‘Synthesis and characterization of various surfactants for stabilized CuO powder’, Materials Research Proceedings, Vol. 8, pp 52-60, 2018

DOI: https://dx.doi.org/10.21741/9781945291999-6

The article was published as article 6 of the book Powder Metallurgy and Advanced Materials

Content from this work may be used under the terms of the Creative Commons Attribution 3.0 licence. Any further distribution of this work must maintain attribution to the author(s) and the title of the work, journal citation and DOI.

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