Microstructure evolution during high cycle fatigue in a low carbon micro-alloyed dual-phase steel sheet

Microstructure evolution during high cycle fatigue in a low carbon micro-alloyed dual-phase steel sheet

Gaurav Pandey, Basudev Bhattacharya, Somjeet Biswas

Abstract. Ferrite–martensite dual-phase (FMDP) steel sheets processed by cold rolling followed by intercritical annealing and quenching were subjected to high-cycle fatigue (HCF) testing to investigate fatigue-induced microstructural evolution. Fatigue tests were conducted at stress amplitudes of 485–580 MPa, and the resulting microstructural changes were examined using SEM and EBSD. The specimen tested at 485 MPa, corresponding to the endurance limit, exhibited a stable microstructure with negligible plastic strain localization. In contrast, higher stress amplitudes led to the formation of persistent slip bands, microcrack initiation at ferrite–martensite interfaces, grain refinement, and significant increases in crystallographic misorientation. EBSD-based GOS, LAM, and KAM analyses revealed enhanced dislocation accumulation and localized plastic deformation at higher stress levels, correlating well with accelerated fatigue damage and premature failure.

Keywords
Dual Phase (DP) Steel, High Cycle Fatigue (HCF), Microstructure Evolution, EBSD, Crystallographic Texture, Damage Mechanism

Published online 5/10/2026, 7 pages
Copyright © 2026 by the author(s)
Published under license by Materials Research Forum LLC., Millersville PA, USA

Citation: Gaurav Pandey, Basudev Bhattacharya, Somjeet Biswas, Microstructure evolution during high cycle fatigue in a low carbon micro-alloyed dual-phase steel sheet, Materials Research Proceedings, Vol. 65, pp 51-57, 2026

DOI: https://doi.org/10.21741/9781644904138-8

The article was published as article 8 of the book Processing and Characterization of Materials

Content from this work may be used under the terms of the Creative Commons Attribution 3.0 license. Any further distribution of this work must maintain attribution to the author(s) and the title of the work, journal citation and DOI.

References
[1] A.H. Steels, September 2016 Application Guidelines, (2016).
[2] Y. Mazaheri, A.H. Jahanara, M. Sheikhi, A.G. Kalashami, High strength-elongation balance in ultrafine grained ferrite-martensite dual phase steels developed by thermomechanical processing, Materials Science and Engineering: A 761 (2019) 138021. https://doi.org/10.1016/j.msea.2019.06.031.
[3] Y. Mazaheri, A. Kermanpur, A. Najafizadeh, A novel route for development of ultrahigh strength dual phase steels, Materials Science and Engineering: A 619 (2014) 1–11. https://doi.org/10.1016/j.msea.2014.09.058.
[4] A.K. Singh, D.K. Chouhan, B. Bhattacharya, S. Biswas, High strength-ductility combination by quenching and partitioning of a low carbon microalloyed dual-phase steel, Materials Science and Engineering: A 870 (2023) 144854. https://doi.org/10.1016/j.msea.2023.144854.
[5] A.K. Singh, B. Bhattacharya, S. Biswas, High strength, ductility and sheet formability by normalizing and quenching of low carbon microalloyed dual-phase steel, Materials Science and Engineering: A 890 (2024) 145848. https://doi.org/10.1016/j.msea.2023.145848.
[6] S. Yan, X. Liu, W.J. Liu, T. Liang, B. Zhang, L. Liu, Y. Zhao, Comparative study on microstructure and mechanical properties of a C-Mn-Si steel treated by quenching and partitioning (Q&P) processes after a full and intercritical austenitization, Materials Science and Engineering A 684 (2017) 261–269. https://doi.org/10.1016/j.msea.2016.12.026.
[7] H. Ashrafi, M. Shamanian, R. Emadi, N. Saeidi, A novel and simple technique for development of dual-phase steels with excellent ductility, Mater. Sci. Eng. A 680 (2017) 197–202, https://doi.org/10.1016/j.msea.2016.10.098.
[7] G.T. Zhang, N.Q. Zhu, B.W. Sun, Z.Z. Zhao, Z.W. Zheng, D. Tang, L. Li, Effect of v addition on microstructure and mechanical properties in c–mn–si steels after quenching and partitioning processes, Metals (Basel) 11 (2021). https://doi.org/10.3390/met11081306.
[8] P. Ghosal, A. Raj, S.K. Paul, Influence of uniaxial and biaxial pre-straining on the low cycle fatigue performance of DP590 steel, Int. J. Fatigue 149 (2021) 106260, https://doi.org/10.1016/j.ijfatigue.2021.106260.
[9] A.M. Sherman, R.G. Davies, The effect of martensite content on the fatigue of a dual-phase steel, Int. J. Fatigue 3 (1981) 36–40, https://doi.org/10.1016/0142- 1123(81)90047-5.
[10] P.C. Chakraborti, M.K. Mitra, Microstructural response on the room temperature low cycle fatigue behaviour of two high strength duplex ferrite–martensite steels and a normalized ferrite–pearlite steel, Int. J. Fatigue 28 (2006) 194–202, https:// doi.org/10.1016/j.ijfatigue.2005.06.024.
[11] M.J. Molaei, A. Ekrami, The effect of dynamic strain aging on fatigue properties of dual phase steels with different martensite morphology, Mater. Sci. Eng. A 527 (2009) 235–238, https://doi.org/10.1016/j.msea.2009.08.005.
[12] G.E. Dieter, D. Bacon, Mechanical Metallurgy 3, McGraw-Hill, New York, 1976, pp. 43–53.
[13] Y. Dai, S. Wang, Q. He, C. Liu, X. Wang, X. Li, L. Li, Y. Liu, C. He, Q. Wang, Effect of microstructure on slip-induced crack initiation and early propagation of martensitic steel during high cycle fatigue, Int. J. Fatigue 167 (2023) 107275, https://doi.org/10.1016/j.ijfatigue.2023.107275.
[14] D. Yu, D. Zhang, Y. Luo, J. Sun, J. Xu, F. Pan, Microstructure evolution during high cycle fatigue in Mg-6Zn-1Mn alloy, Mater. Sci. Eng. A 658 (2016) 99–108, https:// doi.org/10.1016/j.msea.2016.01.061.