Semi-solid thixoforming, microstructure, and mechanical properties of Al-6wt%Si alloy via liquid reaction sintering of elemental powders
Hu Lianxi, Liu Wenchao, Sun Yu, Ba Meiyi
Abstract. Al-6wt%Si semi-solid alloy billets were prepared via the liquid phase reaction sintering process by using elemental Al and Si powders as starting materials. Cup-shaped components were fabricated by direct semi-solid thixoforming at 685-595℃ with the liquid phase fraction in the range of 0.141-0.196. By microstructure observation and mechanical testing, the influence of the liquid phase sintering and subsequent thixoforming conditions on the microstructure evolution and mechanical properties of the final components was investigated. The results show that, when the liquid phase fraction of the alloy billet is in the range of 0.141-0.167, cup-shaped components with uniform microstructure and no forming defects can be obtained by direct thixoforming. Due to the strengthening effect of the fine Al grains and the Si particles and precipitates, the component thixoformed by using billet with a liquid phase fraction of 0.167 presented the best mechanical properties, with yield strength, ultimate tensile strength and elongation achieving 115MPa, 220MPa and 38%, respectively. It is evident that the semi-solid thixoforming process proposed in the present study turns out to be a practical way to fabricate high-performance Al-Si alloy components.
Keywords
Al-Si Alloy, Liquid Reaction Sintering, Semi-Solid Thixoforming, Microstructure Evolution, Mechanical Properties
Published online 5/7/2025, 7 pages
Copyright © 2025 by the author(s)
Published under license by Materials Research Forum LLC., Millersville PA, USA
Citation: Hu Lianxi, Liu Wenchao, Sun Yu, Ba Meiyi, Semi-solid thixoforming, microstructure, and mechanical properties of Al-6wt%Si alloy via liquid reaction sintering of elemental powders, Materials Research Proceedings, Vol. 54, pp 2021-2027, 2025
DOI: https://doi.org/10.21741/9781644903599-217
The article was published as article 217 of the book Material Forming
Content from this work may be used under the terms of the Creative Commons Attribution 3.0 license. Any further distribution of this work must maintain attribution to the author(s) and the title of the work, journal citation and DOI.
References
[1] W Qu, D Li, F Zhang. Multiphase modelling of the transient flow forSn-15Pb and 3570 alloys in semi-solid die casting process, J Mater Process Tech. 278 (2020) 116534. https://doi.org/10.1016/j.jmatprotec.2019.116534
[2] Y G Wang, Q T Guo, N Ren, W Zhang. Experimental and simulation studies of layer casting on industrial-scale Al-4.5wt Pct Cu ingot: Effect, defect, and optimization, J Mater Process Tech. 32 (2003) 118205. https://doi.org/10.1016/j.jmatprotec.2023.118205
[3] Flemings M C. Behavior of metal alloys in the semisolid state, Metallurgical Transactions B. 22 (1991) 269-93. https://doi.org/10.1007/BF02651227
[4] M Kiuchi, R Kopp. Mushy/Semi-Solid Metal Forming Technology-Present and Future, CIRP Annals. 51 (2002) 653-70. https://doi.org/10.1016/S0007-8506(07)61705-3
[5] Z Zhao, Q Chen, Y Wang. Microstructural evolution of an ECAE-formed ZK60-RE magnesium alloy in the semi-solid state, Mat Sci Eng A-Struct. 506 (2009) 8-15. https://doi.org/10.1016/j.msea.2008.12.042
[6] H Takagi, Y Uetani, M Dohi. Effects of Mechanical Stirring and Vibration on the Microstructure of Hypereutectic Al-Si-Cu-Mg Alloy Billets, Materials Transactions.48 (2007) 960-6. https://doi.org/10.2320/matertrans.48.960
[7] D Liu, H V Atkinson, H Jones. Thermodynamic prediction of thixoformability in alloys based on the Al-Si-Cu and Al-Si-Cu-Mg systems, Acta Materialia. 53 (2005) 3807-19. https://doi.org/10.1016/j.actamat.2005.04.028
[8] H Khosravi, R Eslami-Farsani, M Askari-Paykani. Modeling and optimization of cooling slope process parameters for semi-solid casting of A356 Al alloy, T Nonferr Metal Soc. 24 (2014) 961-968. https://doi.org/10.1016/S1003-6326(14)63149-6
[9] S G Shabestari, M Abdi, S Naghdali. Effect of thixoforming and precipitation hardening on microstructure and mechanical properties of Al-10.5Si-3Cu-0.2Mg alloy produced by strain induced melt activation process, J Mater Res Technol. 15 (2021) 4981-4992. https://doi.org/10.1016/j.jmrt.2021.10.086
[10] A Bolouri, C G Kang. Correlation between solid fraction and tensile properties of semisolid RAP processed aluminum alloys, J Alloy Compd. 516 (2012) 192-200. https://doi.org/10.1016/j.jallcom.2011.12.045
[11] B Shayegh Boroujeny, M R Ghashghaei, E Akbari. Effects of SIMA (Strain Induced Melt Activation) on microstructure and electrochemical behavior of Al-Zn-In sacrificial anodes, J Alloy Compd. 731 (2018) 354-63. https://doi.org/10.1016/j.jallcom.2017.09.316
[12] W C Liu, Y Sun, L X Hu. Microstructural properties, thermodynamics and kinetics of Al-Si semi-solid billet fabricated by liquid phase reaction sintering, J Alloy Compd. 885 (2021) 160932. https://doi.org/10.1016/j.jallcom.2021.160932
[13] W C Liu, L X Hu, et al. Microstructure evolution and mechanical properties of Al-8wt.%Si semi-solid billet fabricated by powder metallurgy liquid phase reaction sintering, Materials Science & Engineering A. 802 (2021) 140656. https://doi.org/10.1016/j.msea.2020.140656
[14] W C Liu, L X Hu, et al. Cu strengthened Al-Si-Cu semi-solid billet fabricated by liquid phase reaction sintering, Materials Characterization. 188 (2022) 111925. https://doi.org/10.1016/j.matchar.2022.111925
[15] W C Liu, Preparation via liquid phase reaction sintering and thixoforming of semi-solid Al-Si alloy, Ph. D thesis, Harbin Institute of Technology, 2023