Microstructure, strain rate, and temperature effects on the compressive loading behavior of (FeMnNiCo)1-xMox high entropy alloy

Microstructure, strain rate, and temperature effects on the compressive loading behavior of (FeMnNiCo)1-xMox high entropy alloy

KRÜGER Lutz, CICHOCKI Kamil, HENSCHEL Sebastian, CHULIST Robert, BAŁA Piotr, MUSZKA Krzysztof

download PDF

Abstract. High entropy alloys based on FeMnNiCoMo offer a potential for high energy absorption and high strength, even at low temperatures. In this work, the effects of chemical composition and grain size on the mechanical properties were investigated. Compression tests at a wide range of strain rates and temperatures have been performed. For a strain rate of about 102 s−1 an instrumented drop weight tower was applied. Furthermore, cryogenic temperature tests at −196 °C were carried out. The microstructure was analyzed by means of scanning electron microscopy and transmission Kikuchi diffraction. Hence, the role of grain size, precipitations, and twinning-induced plasticity (TWIP) on the yield strength and the further strain hardening were investigated.

Keywords
High Entropy Alloy, Strain Rate Effect, Temperature Effect, Compression Test, Strain Hardening, Microstructure, Twinning

Published online 9/15/2024, 9 pages
Copyright © 2024 by the author(s)
Published under license by Materials Research Forum LLC., Millersville PA, USA

Citation: KRÜGER Lutz, CICHOCKI Kamil, HENSCHEL Sebastian, CHULIST Robert, BAŁA Piotr, MUSZKA Krzysztof, Microstructure, strain rate, and temperature effects on the compressive loading behavior of (FeMnNiCo)1-xMox high entropy alloy, Materials Research Proceedings, Vol. 44, pp 402-410, 2024

DOI: https://doi.org/10.21741/9781644903254-44

The article was published as article 44 of the book Metal Forming 2024

Content from this work may be used under the terms of the Creative Commons Attribution 3.0 license. Any further distribution of this work must maintain attribution to the author(s) and the title of the work, journal citation and DOI.

References
[1] B. Cantor, I. Chang, P. Knight, A. Vincent, Microstructural development in equiatomic multicomponent alloys, Mat. Sci. Eng. A 375-377 (2004) 213–218. https://doi.org/10.1016/j.msea.2003.10.257
[2] J.-W. Yeh, S.-K. Chen, S.-J. Lin, J.-Y. Gan, T.-S. Chin, T.-T. Shun, C.-H. Tsau, S.-Y. Chang, Nanostructured High‐Entropy Alloys with Multiple Principal Elements: Novel Alloy Design Concepts and Outcomes, Adv. Eng. Mater. 6 (2004) 299–303. https://doi.org/10.1002/adem.200300567
[3] E.P. George, W.A. Curtin, C.C. Tasan, High entropy alloys: A focused review of mechanical properties and deformation mechanisms, Acta Mater. 188 (2020) 435–474. https://doi.org/10.1016/j.actamat.2019.12.015
[4] Z. Li, K.G. Pradeep, Y. Deng, D. Raabe, C.C. Tasan, Metastable high-entropy dual-phase alloys overcome the strength-ductility trade-off, Nature 534 (2016) 227–230. https://doi.org/10.1038/nature17981
[5] M.A. Meyers, O. Vöhringer, V.A. Lubarda, The onset of twinning in metals: a constitutive description, Acta Mater. 49 (2001) 4025–4039. https://doi.org/10.1016/S1359-6454(01)00300-7
[6] S. Basu, Z. Li, K. G. Pradeep, D. Raabe, Strain Rate Sensitivity of a TRIP-Assisted Dual-Phase High-Entropy Alloy, Front. Mater. 5 (2018). https://doi.org/10.3389/fmats.2018.00030
[7] A. Huang, S.J. Fensin, M.A. Meyers, Strain-rate effects and dynamic behavior of high entropy alloys, J. Mater. Res. Technol. 22 (2023) 307–347. https://doi.org/10.1016/j.jmrt.2022.11.057
[8] L.W. Meyer, N. Herzig, T. Halle, F. Hahn, L. Krüger, K.P. Staudhammer, A basic approach for strain rate dependent energy conversion including heat transfer effects: An experimental and numerical study, J. Mater. Process. Tech. 182 (2007) 319–326. https://doi.org/10.1016/j.jmatprotec.2006.07.040
[9] Z. Li, S. Zhao, R.O. Ritchie, M.A. Meyers, Mechanical properties of high-entropy alloys with emphasis on face-centered cubic alloys, Prog. Mater Sci. 102 (2019) 296–345. https://doi.org/10.1016/j.pmatsci.2018.12.003
[10] J.M. Park, J. Moon, J.W. Bae, M.J. Jang, J. Park, S. Lee, H.S. Kim, Strain rate effects of dynamic compressive deformation on mechanical properties and microstructure of CoCrFeMnNi high-entropy alloy, Mat. Sci. Eng. A 719 (2018) 155–163. https://doi.org/10.1016/j.msea.2018.02.031
[11] K. Cichocki, P. Bała, T. Kozieł, G. Cios, N. Schell, K. Muszka, Effect of Mo on Phase Stability and Properties in FeMnNiCo High-Entropy Alloys, Metall. Mater. Trans. A 53 (2022) 1749–1760. https://doi.org/10.1007/s11661-022-06629-x
[12] S. Henschel, L. Krüger, Dynamic crack initiation measurements in a four-point split Hopkinson bending device, Eng. Fract. Mech. 133 (2015) 62–75. https://doi.org/10.1016/j.engfracmech.2015.05.020