Crystallographic Structure Study of a Japanese Sword Masamitsu made in the 1969 using Pulsed Neutron Imaging
Kazuma Ohmae, Yoshiaki Kiyanagi, Hirotaka Sato, Kenichi Oikawa, Anh Hoang Pham, Kenichi Watanabe, Yoshihiro Matsumoto, Takenao Shinohara, Tetsuya Kai, Stefanus Harjo, Masato Ohnuma, Shigekazu Morito, Takuya Ohba, Akira Uritani, M. Ito
download PDFAbstract. Energy-resolved neutron transmission imaging technique using an accelerator-driven pulsed neutron source and a time-resolved two-dimensional detector can obtain the Bragg-edge transmission spectrum at each pixel. In this technique, crystallographic information can be visualized over a wide area of a sample. We used this method to investigate the crystallographic information of a modern Japanese sword produced by Masamitsu in 1969. As a result, shifting and broadening of the (110) Bragg-edge was confirmed at the cutting-edge side. It is evidence that the martensite phase exists at the cutting-edge side as a result of the quenching process. By comparing with results of the old Japanese swords, it is found that the martensite region in the modern Japanese sword is wider or deeper than one in the old swords. In addition, we can see strongly preferred orientation of the crystal grains at the boundary between the martensite phase on the cutting-edge side and the ferrite phase on the back-edge side.
Keywords
Japanese Sword, Masamitsu, Martensite, Crystallographic Structure, Pulsed Neutron Imaging, Bragg-Edge Transmission, RITS Code
Published online 1/5/2020, 6 pages
Copyright © 2020 by the author(s)
Published under license by Materials Research Forum LLC., Millersville PA, USA
Citation: Kazuma Ohmae, Yoshiaki Kiyanagi, Hirotaka Sato, Kenichi Oikawa, Anh Hoang Pham, Kenichi Watanabe, Yoshihiro Matsumoto, Takenao Shinohara, Tetsuya Kai, Stefanus Harjo, Masato Ohnuma, Shigekazu Morito, Takuya Ohba, Akira Uritani, M. Ito, Crystallographic Structure Study of a Japanese Sword Masamitsu made in the 1969 using Pulsed Neutron Imaging, Materials Research Proceedings, Vol. 15, pp 227-232, 2020
DOI: https://doi.org/10.21741/9781644900574-35
The article was published as article 35 of the book Neutron Radiography
Content from this work may be used under the terms of the Creative Commons Attribution 3.0 licence. Any further distribution of this work must maintain attribution to the author(s) and the title of the work, journal citation and DOI.
References
[1] F. Salvemini, F. Grazzi, S. Peetermans, et al., Quantitative characterization of Japanese ancient swords through energy-resolved neutron imaging. J. Analytical Atomic Spectrometry 2012, 27, 1494-1501. https://doi.org/10.1039/c2ja30035d
[2] A. Fedrigo, M. Strobl, A.R. Williams, et al., Neutron imaging study of ‘pattern-welded’ swords from the Viking Age, Archaeol. Anthropol. Sci., 2018, 10, 1249 – 1263. https://doi.org/10.1007/s12520-016-0454-5
[3] Y.Shiota, H. Hasemi, Y. Kiyanagi, Crystallographic analysis of a Japanese sword by using Bragg edge transmission spectroscopy, Phys. Procedia 2017, 88, 128–133. https://doi.org/10.1016/j.phpro.2017.06.017
[4] T. Shinohara, T. Kai, K. Oikawa, et al., Final design of the Energy-Resolved Neutron Imaging System “RADEN” at J-PARC. J. Phys. Conf. Ser. 2016, 746, 012007. https://doi.org/10.1088/1742-6596/746/1/012007
[5] M. Shoji, S. Uno, T. Uchida, et al., Development of GEM-based detector for thermal neutron, J. Inst., 2012, 7, C05003. https://doi.org/10.1088/1748-0221/7/05/C05003
[6] H. Sato, T. Kamiyama, Y. Kiyanagi, A Rietveld-type analysis code for pulsed neutron Bragg-edge transmission imaging and quantitative evaluation of texture and microstructure of a welded α-iron plate. Mater. Trans. 2011, 52, 1294–1302. https://doi.org/10.2320/matertrans.M2010328
[7] H. Sato, T. Sato, Y. Shiota, et al., Relation between Vickers Hardness and Bragg-Edge Broadening in Quenched Steel Rods Observed by Pulsed Neutron Transmission Imaging. Mater. Trans. 2015, 56, 1147-1152. https://doi.org/10.2320/matertrans.M2015049
[8] K. Oikawa, Y. Kiyanagi, H. Sato, et al., Pulsed neutron imaging based crystallographic structure study of a Japanese sword made by Sukemasa in the Muromachi period, Mater. Res. Proc. (this proceedings).
[9] H. Sato, Y. Kiyanagi, K. Oikawa, et al., Crystallographic microstructure study of a Japanese sword made by Noritsuna in the Muromachi period by pulsed neutron Bragg-edge transmission imaging, Mater. Res. Proc. (this proceedings).